ASTM F2013-10 (2016) Standard Test Method for Determination of acetaldehyde Residues in polyethylene terephthalate Bottle Polymers Using an Automatic Static Headspace Sampling Device and Capillary Gas Chromatograph with a Flame Ionization Detector is especially used as a quality control tool for molding or synthesis operations.

Arti dan kegunaannya

5.1 This test method is especially used as a quality control tool for molding or synthesis operations. Acetaldehyde is a volatile degradation product produced during PET melting processing. Sebagai akibat, it is captured in the side wall of the molded product and slowly desorbed into the contents packaged therein. In some foods and beverages, AA can give off an undesirable taste, so it is important to understand its concentration in PET products used in food contact applications.

ASTM F2013-2016 Metode Uji Standar Penentuan Residu Asetaldehida pada Polimer dari Botol Polietilen Tereftalat Menggunakan Alat Pengambil Sampel Headspace Statis Otomatis dan Kromatografi Gas Kapiler dengan Detektor Ionisasi Api

5.2 Desorption conditions at 150°C for 60 minutes should ensure that no measurable AA is produced in the sample during desorption.

Melangkah 1: Cakupan

1.1 This test method covers gas chromatography for the determination of ppm residual acetaldehyde (AA) in polyethylene terephthalate (PELIHARAAN) homopolymers and copolymers used in beverage bottle production. This includes sample types for amorphous and solid particle samples and billet samples, as opposed to bottling tests (test method D4509), which require 24 hours of desorption into the top space of the bottle at 23°C before concentration. Headspace was quantified by a similar GC method.

1.2 Nilai yang dinyatakan dalam satuan SI dianggap sebagai nilai standar. This standard does not include other units of measurement.

1.3 Standar ini tidak dimaksudkan untuk mengatasi semua masalah keselamatan yang terkait dengan penggunaannya. It is the responsibility of the user of this standard to establish appropriate safety and health measures prior to use and to determine the applicability of regulatory restrictions.

ASTM F2013-2016 Metode Uji Standar Penentuan Residu Asetaldehida pada Polimer dari Botol Polietilen Tereftalat Menggunakan Alat Pengambil Sampel Headspace Statis Otomatis dan Kromatografi Gas Kapiler dengan Detektor Ionisasi Api

2. Lihat berkasnya

standar ASTM

D4509 Test method for the determination of acetaldehyde content in the 24-hour gas (AIR) space in newly blown PET bottles

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