序文
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この文書を担当する委員会は ISO/TC です。 256, 顔料, Dyes and increments.

ISO 18473 consists of the following parts under the general heading Functional pigments and increments for special applications:

— 一部 1: Nanometer calcium carbonate for sealant applications

— 一部 2: Nanoscale titanium dioxide for sunscreen applications

ISO 18473-1-2015 特殊用途向けの機能性顔料・フィラー – 一部 1: シーラント用途向けのナノサイズ炭酸カルシウム

導入
Sealants are widely used to prevent air, gas or liquid infiltration into many industries, 建設も含めて, automobiles and electronics. Increments are an important component of sealant formulations that reduce cost and improve rheological and mechanical properties. The content of increment agent varies widely and can be as high as 50% (mass fraction). A common additive in sealants is calcium carbonate (CaCO 3) because it is readily available in a variety of sizes and can be used as a rheological modifier, enhancer, and sunblock. Commercial calcium carbonate can be divided into heavy calcium carbonate (GCC) and precipitated calcium carbonate (PCC), with three crystal structures of calcite, aragonite and spheroid aragonite. It exists in various forms, such as cubic, spherical, spindle, fibrous and acicular. Calcium carbonate with calcite crystal structure and cubic or spherical form is most widely used in sealant applications.

Nanoscale calcium carbonate (NCC) provides improved performance and additional features for a variety of sealants, including thixotropy, flame retardant, and improved durability and recyclability, and has become a major ingredient in sealant formulations. Nanoscale calcium carbonate in powder form is now easy to manufacture, mainly through the precipitation route to control size and form. The importance of surface treatment for the use of NCC in sealants cannot be overstated. Natural calcium carbonate 3 is hydrophilic. 結果として, it tends to clump in organic polymers and plasticizers. NCCS, in particular, tend to aggregate more easily due to their small size and large surface area. NCCS are surface treated to give them hydrophobicity and improve their dispersion in hydrophobic systems. The surface treatment also improves the compatibility of the polymer matrix, thus improving the interface adhesion between the increment agent and the polymer.

It was found that the particle size, 比表面積, mass fraction, morphology, pH値, magnesium content, oil absorption value, water content and other characteristics of the supplied nano-sized calcium carbonate affected the performance of the sealant mixed with these materials. Nanoparticles. The characteristics of NCCS that need to be detailed in relation to sealant performance arise from the following facts. 初め, agreements between customers and suppliers do not always cover all material characteristics that affect sealant performance and/or machinability, or they are interpreted differently by customers and suppliers. 2番, nanomaterials are relatively new. Material properties may depend on the technique used to measure them. So,

ISO のこの部分 18473 lists the properties, measurements and characteristics of nanoscale calcium carbonate and is intended to aid its acceptance and application in sealants.

1 適用範囲
ISO のこの部分 18473 specifies the requirements and corresponding test methods for powdered nano-sized calcium carbonate for surface treatments used in sealant applications.

2 規範的な参照ファイル
All or part of the following documents are conventionally referenced in this document and are required for the application of this document. 日付の付いた参照については, 引用のみのバージョンが適用されます. 日付のない引用については, 参照ドキュメントの新しいバージョン (修正も含めて) 当てはまる.

ISO 787-2, General test methods for pigments and increments-Part 2: Determination of volatiles at 105 ℃

ISO 787-5, General test methods for pigments and increments – 一部 5: Determination of oil absorption values

ISO 787-9, General test methods for pigments and increments-Part 9: Determination of the pH value of aqueous suspensions

ISO 3262-1, coating increments — 仕様と試験方法 — 一部 1: Introduction and general test methods

ISO 3262-6, paint increments-specification and test methods-Part 6: Precipitated calcium carbonate

– ISO 9277, ガス吸着による固体の比表面積の測定 – BET方式

ISO 15528, 塗料, ワニスおよび塗料およびワニスの原料 – サンプリング

ISO 18473-1-2015 特殊用途向けの機能性顔料・フィラー – 一部 1: シーラント用途向けのナノサイズ炭酸カルシウム

3 用語と定義
For the purposes of this part of ISO 18473, 次の用語と定義が適用されます.

3.1 Nanoscale

サイズの範囲はおよそからです 1 nmから 100 nm

エントリーノート 1: Attributes that are not extrapolated from a larger size are usually (but not limited to) displayed within this size range. For such attributes, the size limit is considered to be approximate.

エントリーノート 2: The lower limit in this definition (approximately 1 nm) was introduced to avoid the designation of individual and small atomic groups as nanoobjects or nanostructured elements, which may imply that there is no lower limit.

3.2 Precipitate calcium carbonate

A synthetic calcium carbonate composed of triangular crystals (例えば, 方解石) or diamond-shaped biconical crystals (例えば, aragonite)

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