意义和目的
The test method in this standard can be used to measure U in 99Tc, 230钍, 和 234 soil samples. The test method is applicable to soils contaminated by nuclear-related activities such as uranium ore processing and uranium enrichment. The FI concentration step can reduce the detection limit by about 10 times compared to ICP-MS introduced for conventional samples. The approximate IDL is listed in Table 1.

范围
1.1 This test method includes measurement procedure 99Tc and measurement procedure 230 days and 234U in the soil. Applicable to background soils and soils contaminated by nuclear processes. It is intended as an alternative to radiochemical methods as it is faster, requires less labor, and produces less waste than many radiochemical methods.

1.2 The samples were dried, 地面, melted and dissolved, and analyzed by inductively coupled plasma mass spectrometry (ICP-MS). Sequential flow injection (FI) technology is used to provide a lower detection limit than that obtained by direct inhalation ICP-MS and, at 99Tc, to provide isolation from interference.

这 1.3230 day and 234U procedures also work for 232Th, 235U, and 238U, but FI preenrichment is generally not required to measure these isotopes at the concentrations typically found in soil.

美国材料试验协会D 1310-01-2007 “泰格开瓶器测定液体的闪点和燃点”

1.4 This test method is guided by SW-846 and the quality control procedures derived from the U.S. EPA Inorganic Analysis Program as reported in the Contract Laboratory Program Work Instructions. The level of quality control required may vary from laboratory to laboratory and project to project. Laboratory statistical quality control procedures are required to ensure the reliability of this test method.

1.5 becquerels (Bq) is an acceptable metric unit of radionuclide activity. 然而, picocuries (pCi) are generally the units used to represent regulatory limits for radioactivity. Values expressed in any of these units should be considered standard values. 每个系统中指定的值可能不完全相同; 因此, each system needs to be used independently of the other, rather than combining values in any way.

1.6 Refer to Practice C 998 for information on soil sample collection.

1.7 本标准并非旨在解决所有安全问题, 如果有的话, 与其使用相关. 本标准的使用者有责任建立适当的安全和健康实践，并在使用前确定监管限制的适用性.